SIZE DISTRIBUTIONS OF RADIOACTIVE AEROSOLS

161

for total beta measurement on miniature thin-wall Geiger counters
whose backgrounds were about 0.2 count/min with 20-cm-steel and
anticoincidence shielding.® Filters were measured for total beta activity
on a larger Geiger counter of identical design with identical shielding
with a background of about 6 counts/min. All total beta counting

rates were normalized by multiplying by factors of 3.44 (miniatur

counter and 3.09 (large counter) to correct for geometry (G). Beta.
absorption differences between the two counters were considered
to be negligibly small. For total gamma measurements (0.1 to 1.0

Mev), card-mounted stages 1 and 2
(2.5 cm in diameter by 1.3 cm in
8-cm Nal(Tl) crystal located within
distance between the crystal surface

samples and pelletized filters
height) were placed on an 8- by
10 cm of lead shielding. The
and the card-mounted sam-

ples was about 0.6 cm. Filter counting rates were normalized to those

of stages 1 and 2 samples by anincrease of 40% to correct for geometry
differences. Samples were then dissolved from the tape and the filter
by digestion with aqua regia in the presence of appropriate carriers.
Individual radionuclides were separated and purified by standard radiochemical procedures. All beta-activity measurements for the de-

termination of Sr, Zr, MOR, and '4Ce were made on miniature

Geiger counters by using the Libby thick-solid-sample technique,’
and radionuclides were identified by either beta-particle absorption
in aluminum or by decay. Corrections for counter background, geometry,
self-absorption, and external absorption were made in converting counts
per minute into disintegrations per minute. For “Mn measurements

the 0.84-Mev gamma ray was counted, and all gamma-counting data
were recorded on a multichannel analyzer. Individual radionuclide
concentrations in units of disintegrations per minute per cubic meter

[S.T.P. (0°C and 760 mm Hg)] were obtained by using volume data
provided by GMI.

RESULTS AND GENERALDISCUSSION
Sampling data for the impactor—filter collections for the four
balloon flights are given in Table 1. Although there are slight variations, the sampling-altitude intervals will be considered to be 9 to 15,

15 to 21, 21 to 27, and 27 to 30 km, and the particle cutoff sizes will be
considered to be 0.15 and 0.02 in radius for stages 1 and 2, respec-

tively.
Table 2 lists our sampling dates relative to announced atmospheric

nuclear tests whose fission yields were at least about 1 Mt. Time
intervals between the last reported test of at least this size and our
sampling dates are 132, 145, and 236 days for collections of March
1962, May 1963, and August 1963, respectively. In each of these cases,

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