TABLE 5.2
Predicted vs Observed Particle Size Separations by Stendard Sleves
Size Range of Sieves
Cry
$3
53-62

dy
fon
.

74-88
88-105
105-125
125-149

62.4
&s.8
113
116
172
215

159-177

Number of Particles
Sounted

239

321
228

.

369
150
181
381

__186

The frection from the 62-74 pp sieve hed a particularly broad

distribution, so that all data associated with it should be viewed
with great suspicion.

The Roller analyzer, used here for particles smaller than 50 p,

provides sharper size separations less sensitive to particle shape

than the sieves.

On the other hand it is more likely to break up

frengible or agglomerated particles.
A comparison of czlibrated size
with observed size is given in Table 5.3.

TARLE 5.3
Predicted vs Observed Particle Size Separations by Roller Analyzer

Calibrated

Size Range

(p)

0-5
5-10
10-20
20-30
20-40

ay

Number of

(yp)

Particles

Counted

5.08
10.3
23.3
29.5
43,7

“He
743
376
1089
429

From recent autoradiographic studies it has been found that the
experimental determination of the per cent active particles in the
lower size range may require a correction under certain conditions.*

This results fron experimental limitations as to the size and specific

activity of a particle which mzy be cetected as hot.

*This discussion of autoradiograph errors is due to Mr. Robert J.
“French of these Laboratories,

38

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