Meetings have been held over the past six months relative to the selection of
nuclear sites for intensive study.
areas are under analysis.

Preliminary samples from the nonclassified

AREAS OF CONCERN AND RECOMMENDATIONS

The LASL soil study personnel have reviewed past and recent activities as they
relate to initial assignment. A primary purpose for the review has been to
indicate major problems which require further study.
By way of summary,
recognized gaps in our knowledge are presented as questions, answers, and

recommendations from the LASL soil studies personnel and other NAEG principal
investigators who have indicated to us related problems.
Sampling

For the soil types sampled, data indicate that if cross contamination has

occurred, it has not contributed significantly to the results presented.

For

the types of soil sampled, the two methods presented, surface and profile
sampling, have been successfully used for the safety shot site soils.
For
stony or rock soils as will be encountered in the nuclear sites, for sampling
into highly cemented soil horizons, or for special matrices such as asphalt,
concrete, steel, or wood, the LASL soil study personnel recommend development
and testing of special sampling techniques.
Groundwater, mucks, and sludges
will present problems, particularly if profile samples are to be required.
Testing procedures should consist of (1) determination of physical uniformity
of samples collected,

(2) measurement of degree of cross contamination due to

sampling, and (3) comparison of methods statistically.

Analytical Methods for Radionuclides of Interest
Of certain radioisotopes listed in the original charter, the major effort has
been placed on plutonium, americium, and uranium.
As related to the original

charge, are the analytical methods now in use or available adequate for the
determination of low levels of activity of future radionuclides of interest?

The methods for plutonium analysis used to date have proved adequate on standard

samples; however, comparison of samples is difficult where the "hot particle
problem" exists.
A concentrated effort should be expended on testing of
present radiochemical procedures for low levels of 24lan, especially where
plutonium to americium ratios are of interest.
The work on such methods now
in progress could serve as a useful base.
Quality Assurance

The LASL soil study personnel view quality assurance as a most essential part
of any sampling and analysis program. A question is posed as to the adequacy
of the present quality assurance program.

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