to this peak

and we

can get

an

accurate number

in disintegrations per

minute of plutonium-239, which effectively gives you picocuries per gram.

A couple of things you should look at in this figure is the resolution
of_the spectra.

If you have plating prob lems or detector problems, these

peaks will get much wider and you will get overlaps and it's difficult to

‘extract the information from them.
50-60 keV, if I remember correctly.
obviously coming from thorium.
interfere ‘signtficant ly with

The resolution here is on the order of
There are other peaks in the spectra,

I wanted you to see that they don't really
the plutonium-239

and

-236.

There

is one

10

smal] interference.

11

Radium-224 has a three-day half-life and it ingrows because it's eliminated

12

in the chemistry, but as soon as you plate it, it starts ingrowing from the

13

thorium.

14

plutonium-236, so we have taaccount for the length of time between the

15

plating and the counting and~the ingrowth of the radium-224 and subtract

16

that from the plutonium-236.

17

tially zero.

18

the thorium-228 peak which gives you an estimate of what kind of error

This thorium-228 has a daughter which is radium-224.

Its peak ties_right here and can create a shoulder

in the

If you do it within a few hours, it's essen-

If you wait several weeks, it can go into the same height as

19
20

One last point.

The reason that youcan't do plutonium-240 this way,

21

and you have to go with the mass spectroscopy is that the energy of the

22

plutonium-240 jis the same as the plutonium-239.

23 - 239 and 240.

I should have written this

The 236 has a different energy but--we are just unlucky in

24

that 239 and 240 have the same alpha energy and you—just_can't discriminate

25

between them.

;

26

That concludes my presentation.

27

CHAIRMAN MOSELEY:

28

DR. WRENN:

Are there any questtons?

Or. Wrenn.

If you do radiochemical

165

separation, why do you have so

Select target paragraph3