analyzed here to perform such an analysis.
309

RADIOACTIVE PARTICLE SIZE ANALYSIS

The dried samples from all trays of each collector were combined,

weighed, and then sieved through a 44-p sieve.

The weight of each

fraction was determined and a weighed portion of each fraction was
used for radioautography.e

These fractions were washed from the weighing dishes with
toluene onto the backside of Eastman NIB stripping film which was previously mounted on 4-in. plastic rings. The transfer was done in dim

light.

Canada balsam, which was added before the toluene evaporated

to form a uniform adhesive medium for the particles,did not interfere
with microscopic observation. The celluloid backing separated the
particles from the emulsion so that during processing the particle

medium was not disturbed (Figs 3029). The NTB film has a 10—p thick

emulsion and a 7p thick backing.
The radioautographs were exposed for the empirically determined
time of 15 hr for samples measuring 100,000 cpm, 25 hr for samples
counting 50,000 cpm, 60 hr for 25,000 cpm, etc. All exposures were
started 6 to 9 days after each shot.

The radioautographs were devel=-

oped in Eastman Kodak D~-19 Developer for 5 min at 20° C., then rinsed

and fixed for 10 min. All develcping operations were done without disturbing the particle medium. The particles were projected at 2 magnification of 1000 times with a micro-projector which consisted of a
Bausch and Lomb research microscope mounted on a micro=projector base

with carbon arc
a megnification
The limitations
particles below

illumination. The particle images we-e projected at
of 1000X. Radioactive particles cnly were measured.
of the optical microscope precluded the observation of
about 1 pe

PARTICLES

i=

BACKING

CANADA BALSAN

TZ) NT
emuLsion

PREPARATION POSITION
SOLUTION

EMULSION

BACKING |
CANADA

PARTICLES

HOLDER

BALSAM

DEVELOPING AND EXAMINATION POSITION

Fige 3029

Preparation of Particle Medium; Developing

and Examination Position of Stripping Film

85

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