UNCLASSIFIED > em om ehmn a e o to e INTRODUCTION A study has been made of the chemical composition, structure and distribution of radioactivity in the radioactive fallout particles resulting from a moderate-yield tower shot in Operation REDWING at the Eniwetok Proving Grounds. fo collect samples of the radioactive fallout, large, open trays were placed on several of the islands which extended along the atoll for a few miles on each side of the shot point. On only one of these islands, approximately ten miles from the shot point, was fallout sufficiently heavy to provide abundant samples of the fallout particles. The trays from this island were picked up, secured for transportation and shipped to this laboratory. In order to study the radioactive fallout particles it was necessary first to separate them from the inactive sand grains which had been swept into the open trays by surface winds. This was done by removing al11 the particles from the trays and sprinkling them onto the backs of pieces of single-~coated X-ray sheet film. Just before dispersing the particles onto the film, the film had been sprayed with a thin layer of liquid plastic which, after hardening, held the scattered particles onto the film. After an exposure of a few hours the films were developed and fixed by brushing the appropriate solutions onto the emulsion side of the film, with care not to disturb the particles on the other side. The radioactive particles were easily identified by the halo of darkened film surrounding them. Many of the radioactive particles were then removed from the films and mounted in small plastic pellets which were then ground into thin sections IMMERRE ee gw with standard petrological techniques. ; These sections, which were cut through the center of each particle, were about 30 p thick. By studying these thin sections under the petrographic microscope it was possible to identify the transparent compounds and to observe the structure of the fallout particles. The opaque compounds in the particles were identified by X-ray diffraction analysis. The distribution of radioactivity within the particles was found by radioautographing the thin sections with Eastman NIB stripping film. I UNCLASSIFITZED — eee ee

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