EZ EEREGAZILTEREDS

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i

the other alkaline earths.(4)

With trsicr tethmioue, a high yield of

carrier strontium can be obtained,

Several ecsid treatments are required

and the actual number depends on the ameunt of calcium which was leached
from the soil,

Following the fumirg nitric acid separation, thorium,

lead and any contaminating fission preducts remaining are scavenged with
yttrium hydroxide, and radium and barium are removed by a barium chromate
precipitation.
The daughter yttrium is milked after equilibrium and beta counted
as a measure of the strontium-90 activity.

Absorption corrections are not

necessary since the weight of the precipitate can be rigidly controlled
at this point.

Twenty milligrams of yttrium carrier are added just prior

to milking and the standards are prepared in an identical manner.

The

step-wise analytical procedure is given in section 6.2 of the Appendix.

Colt

OGLTLE

Samples are mounted on piastic cises, covered with Mylar, and
the assembly secured with a plasti: rioz.

The sample is clamped into

position under one of three oneeinch Anton halogenefilled steel window

GeM tubes (# 1007 M) which are surrounded by a guard ring (46 "pencil
tubes" Anton# 315) in anticoinciderce, shielded with 3 inches of mercury
and beta counted for at least one hour,

FEackgrounds less than one count

per minute are obtained using this counting system. (3)

(i)

Modification of the method reported by Willard, NoHe, and Goodspeed,
Bo Wes

(5)

More recently,

res

Indus oe

ENE o

Chems

Ans?,

mang,

ah (1936),

NYO-h700 @ Manual of Stacti.: © tistives,

LeVine, HeDo, Charlton, Loe, Greviicr, “:t., Low Background Nuclear
Counting Equipment, HASL-650, liars. 25, 1)

Select target paragraph3