t3

Tue decay of “cs milked yttoium-90 has been followed for every sample

analyzed and within two standard deviations due to the error in counting,

e, straight lins representing the established half-life (64.4 hours)? is
always found.

Figure 2 shows seven examples of the decay curves obtained.

In several cases waere the activity has been sufficiently high, the
yttrium-90 fraction has been analyzed by the beta absorption method of
Harley and Haliden.‘?)

The value for the energy found by this method

agreed satisfactorily with that generally accepted (2.26 Mey). (5)
2.8

Compaxison of Extraction Method and Fusion

By fusing an aliquot (1 lb.) of soil with sodium carbonate at
temperatures eround 200° o(9) and then dissolving the melt in mineral
acid, one can solubilize the soll campletely.

If the assumption is made

that the fusion analysis gives the total amount of strontium-90 in the
soil, one can express the fraction or percentage of the total amount of
strontium-90 removed by the hydrochloric acid extraction.
The soil sempiss shown in Table 5 were collected in pasture

areas in the United States in 1956 and 1958. At least ten reanalyses
have been carrisd out on each sample, (1°) The values for a/m sr”? per kg
soil ars averag:s and the error term is one standard deviation from the
mean.

(6) Volchok, H. Ley Kulp, J. Ley Phys. Rev. 97, 102 (1955).

(7) Harley, J. H., and Hallden, N: A., Nucleonics, Jan. 1955, P. 32.
(8) Johnson, 0. E., Johnson, R. G., langer, L. M., Phys. Rev. 98, 1517

(1955).

(9)

This work vas done at the USDA Iaboratories at Beltsville, Md. -under
tne dizvecricnu of Br. L. T. Alexander.

(10) See proceturs given in NYO-4700 - Manual of Standard Procedures.
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