value for m, among other things, depends on the within-laboratory

variability (variability between replicate analyses) and the size of
the actual difference between labs.

Gilbert e¢ al.

(1975) conclude

that for soil samples from the safety-shot sites, the use of only

three replicate analyses per sample by each laboratory is not likely
They suggest that the
ro detect even large differences between labs.
use of less than 10 replicates might be largely a waste of time and
money if one wants a fairly good chance of detecting even a ratio of
Since environmental vegetation
2? between the high and low lab.
samples are presumed to be less affected by the hot particle problem
(the vegetation sample is dissolved, Major e¢ al.,

1974),

the within-

lab variability should be less than for soil samples, allowing the
use of fewer replicate analyses per sample.

Some data is now becoming

available for estimating this within-lab variability for vegetation.
Hopefully, the hot particle problem in soil will not be as great at
the nuclear study sites, allowing for a smaller number m of replicate
analyses per lab.

Since "standard" samples are prepared so that all

aliquots should have the same plutonium concentration, an m of 3 per
laboratory for these samples may not be unreasonable, although we
have yet to examine the question with actual data.

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