.

et

fa. attecal,

All of the values reported by the contractor are corrected for a
reagent biank.

sco

that the blank values reported here refiect

the con-

taminaticn of the filter material both during manufacture and Guring
handling at HASL and at the contractor labcratory.
Table l lists the results of the analyses of the blanks for each
In general these data indicate low levels of contamination

for mest of the nuclides,

however it is significant to note tha

ct

nuclide.

a]

average Pu-238 biank rose from C.0C4 dpm in 1967
Becsuss the amount Of Pu-2383 found in
quently in

the

to 9.22 dom in 1968.

surface air sampies is fre-~

the range of 1 dom this blank may represent a significant

fraction cf the total activity.
The results of analyses on standard samples are shcwn in Table 2.
These

data are indicative of the accuracy cf the radiochemical anal-

yses.

The values shown are the average percert deviaticns between

added activities and the results reported by the contracter.
most of the results are satisfactory,

there appezrs

the

Although

to be a large pesi-

tive bias in the Pu~-238 values fer much of 1968, which cannot be accounted for by the increase of the blank ccntamination.

Samples sub=-

mitted to the contractor during 1969 which were prepared with a new
standard solution do not exhibit this bias,

and it is therefore pre-=

bable that the peor results reflect a degeneration cf the Pu-2338 stardard solution used for the preparation of the 1968 quality control

samples.

T - 10

.

Select target paragraph3